A one-pot synthesis and X-Ray structural characterization of new highly substituted-allyl carbamates

A one-pot synthesis of new variously substituted γ-chloro-γ, β-allylic carbamates have been carried out starting from β-chloro-α, β-unsaturated aldehydes. The and the corresponding intermediates, alcohols, were fully characterized by (1H 13C) NMR, IR HRMS spectroscopic techniques. crystal structures two allylic carbamates, established single-crystal X-ray diffraction.